sso7d [u-13C/15N] 1.7mM in 100mM NaOAc-d3 pH=4. +PIC + antibiotics 4% D2O T=290K
250ul in 5mm shigemi, prepared 20.12.2018
[13C,1H]-HSQC (aliphatic region) gradient-selected, non-sensitivity enhanced NS=4 TD1=320 SW(F1)=71ppm
sso7d_700/4 27.12.2018
using 13C 180deg. BIPs in INEPTs, w/ carbonyl decoupling w/o 15N (plw3=0) decoupling in F1